
New TopShim run:

version = topshim 2.0.0
date = 2024-09-17
time = 20:17:59.660
command = topshim 

FINE SHIMMING

Parameters:

probe = Z168772_0022
solvent = CDCl3
shim nucleus = 2H
nucleus optimised for = 1H
o1p (from lock) = 7.24 ppm

Results:


1D Shimming:
Iteration  1: FWHM Before= 0.7 Hz, Target= 1.4 Hz, After= 2.6 Hz
Iteration  2: FWHM Before= 2.6 Hz, Target= 0.3 Hz, After= 3.8 Hz
Iteration  3: FWHM Before= 3.8 Hz, Target= 0.3 Hz, After= 0.7 Hz
Iteration  4: FWHM Before= 0.7 Hz, Target= 0.3 Hz, After= 2.2 Hz
Iteration  5: FWHM Before= 2.2 Hz, Target= 0.6 Hz, After= 0.4 Hz
Shim succeeded

Lineshape quality factor (1D spectrum, spinning) = 0.909

shim changes: 
Z	-1308
Z2	-603
Z3	-1686
Z4	-8021
Z5	-4147

duration = 4 min 20 sec
completed successfully
finished Tue Sep 17 20:22:18 2024


========================================================================

New TopShim run:

version = topshim 2.0.0
date = 2024-09-17
time = 20:22:30.583
command = topshim  tunea tune

TUNE

Parameters:

probe = Z168772_0022
solvent = CDCl3

Results:


Performing tune after shimming
tune lock level increase = 1.0

shim changes: 
Z	-6
X	-39
XZ	-33
Y	+41
YZ	-2

duration = 1 min 11 sec
completed successfully
finished Tue Sep 17 20:23:40 2024


========================================================================

New TopShim run:

version = topshim 2.0.0
date = 2024-09-17
time = 20:24:02.787
command = topshim 

FINE SHIMMING

Parameters:

probe = Z168772_0022
solvent = CDCl3
shim nucleus = 2H
nucleus optimised for = 1H
o1p (from lock) = 7.24 ppm

Results:


1D Shimming:
Iteration  1: FWHM Before= 0.8 Hz, Target= 0.3 Hz, After= 0.6 Hz
Iteration  2: FWHM Before= 0.6 Hz, Target= 0.3 Hz, After= 1.5 Hz
Iteration  3: FWHM Before= 1.5 Hz, Target= 0.4 Hz, After= 1.3 Hz
Iteration  4: FWHM Before= 1.3 Hz, Target= 0.4 Hz, After= 0.9 Hz
Iteration  5: FWHM Before= 0.9 Hz, Target= 0.4 Hz, After= 1.5 Hz
Iteration  6: FWHM Before= 1.5 Hz, Target= 0.8 Hz, After= 2.2 Hz
Rejecting all results and reverting to the initial shim state.

Lineshape quality factor (1D spectrum, spinning) = 1.35

shim changes: none

duration = 3 min 50 sec
completed successfully
finished Tue Sep 17 20:27:51 2024


========================================================================
